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Beilstein J. Org. Chem. 2012, 8, 1037–1047, doi:10.3762/bjoc.8.116
Graphical Abstract
Scheme 1: β-diketonate complexes (left), homoleptic complexes (middle) and planned homoleptic complexes of eu...
Scheme 2: Pyrrole–pyridine-based structures synthesized in this study.
Scheme 3: Retrosynthetic approach for structures 1–3.
Scheme 4: Synthesis of the heteroaryl bromides used in the coupling reaction.
Scheme 5: Generation of the borate intermediate 21/22.
Scheme 6: In situ Suzuki coupling reactions of the heteroaryl bromides 8–10.
Figure 1: The structure of compound 1 in the crystal. Ellipsoids correspond to 50% probability levels.
Figure 2: Packing diagram of compound 1, viewed parallel to the y-axis in the range y ≈ 1/4. Hydrogen bonds a...
Figure 3: The structure of compound 2·CH3OH in the crystal. Ellipsoids correspond to 50% probability levels. ...
Figure 4: Packing diagram of compound 2·CH3OH showing the formation of inversion-symmetric "stacked" dimers. ...
Figure 5: The structure of compound 3·C2H5OH in the crystal. Ellipsoids correspond to 50% probability levels....
Figure 6: Packing diagram of compound 3·C2H5OH. Hydrogen bonds are shown as thick dashed lines. Hydrogen atom...